29,33,39 On the other hand, hydrogens from the OH group can actively reduce S–S bonds because of their constructive charge. Hence, the hydrogen atom that cuts down the S–S bond can come from the α-carbons or the OH group. The other sulphur atom can sort a C
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If you did an acid/foundation extraction, this stage is most likely unneeded, particularly when you defatted ahead of recovering the freebase. It can be carried out when you’re actually concerned about impurities and aren’t a fan of any of the next purification solutions.
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